The ELEMENTRAC ONH-p determines oxygen, nitrogen and hydrogen in inorganic samples by inert gas fusion in an impulse furnace with temperatures in excess of 3.000 Â°C.
The ELEMENTRAC ONH-p guarantees precise and fast sample analysis. The analyzer covers a wide range of applications such as metal, ceramics and other inorganic materials.
The ELEMENTRAC ONH-p can be supplied with up to two infrared cells with different path lengths, accommodating both high and low level oxygen analyses. Nitrogen and hydrogen concentrations are determined in the ELEMENTRAC ONH-p by a robust and sensitive thermal conductivity cell.
alloys, cast iron, ceramics, copper, refractory metals, steel, ...
|Measured elements||hydrogen, nitrogen, oxygen|
|Sample carrier||graphite crucibles|
|Field of application||ceramics, engineering / electronics, steel / metallurgy|
|Furnace||electrode impulse furnace (max. 8,5 KW*), temperatures in excess of 3,000 °C|
|Detection method||solid state infrared absorption for oxygen thermal conductivity for nitrogen and hydrogen|
|Typical analysis time||120 - 180 s|
|Chemicals required||copper oxide, magnesium perchlorate, Schuetze reagents, sodium hydroxide|
|Gas required||compressed air, helium 99.995 % pure, nitrogen 99.995% pure, argon 99.995% pure (if required), all gases with (2 - 4 bar / 30 - 60 psi)|
|Power requirements||3~ 400 V, 50/60 Hz, max. 8,500 W|
|Dimensions (W x H x D)||57 x 77 x 63 cm|
|Weight||~ 161 kg|
|Required equipment||balance (resolution 0.0001g), monitor, PC|
|Optional accessories||carrier gas purification, external chiller, gas calibration unit|
|* limited to 6.8 kw in application settings|
Operation of the ELEMENTRAC ONH-p is simple and safe. The samples are weighed on the interfaced balance and the weight is transferred to the linked PC. Manual weight entry is also possible.
Depending on the application the sample has to be placed in a nickel basket or capsule. Granulates or pins made of steel can be placed directly on the sample port without any other tools. Some applications require additional fluxes like tin or nickel, which have to be given in an empty graphite crucible. This graphite crucible is placed on the lower electrode tip and then the analysis is started. Typical analysis time is about 2.5 minutes.
All cell outputs and analyzer parameters are displayed in real time and are saved in a data base along with the results. Of course the results and application settings can be exported. The ELEMENTRAC ONH-p requires minimum maintenance and all particle filters and chemicals which need to be maintained are easily accessible. During daily work a door hides chemicals and filters. It can be removed easily to observe these during analysis.
Measuring Principle ELEMENTRAC ONH-p
The measuring principle of the ELEMENTRAC ONH-p allows for a wide measuring range. To analyze the sample, it is weighed and placed on the sample port. Flushing with carrier gas prevents atmospheric gas (oxygen and nitrogen) from getting into the furnace.
The graphite crucible is outgassed in the impulse furnace to reduce possible contaminations (e.g. residual hydrogen). After a stabilization phase the sample is dropped into the crucible and melts. Carbon monoxide is produced by the reaction of carbon in the graphite crucible and oxygen of the sample. Nitrogen and hydrogen are released in its elemental form. The carrier gas (helium) and sample gasses pass through a filter before entering a copper oxide catalyst which converts the CO to CO2.
The CO2 is measured by the infrared cells to determine the oxygen content. CO2 and water are removed chemically and the nitrogen content is measured in the thermal conductivity cell. In the case of hydrogen analysis the nitrogen carrier gas and the sample gas passes through a Schuetze reagent instead of a copper oxide catalyst. As an option the less expensive Argon can be used to determinate the oxygen and nitrogen content.
Subject to technical modifications and errors